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class="NyNewDetail_Content" id="c_detail_wrap"> <div> <strong><a href="http:///jsshengaohua-Products-36206667/" target="_blank">便攜式紅外測(cè)油儀</a></strong>根據(jù)GB16488-1996和HJ637-2012國(guó)家標(biāo)準(zhǔn)，用四氯乙烯萃取水中的油類物質(zhì)，然后使用無(wú)水硫酸鈉隔離雜質(zhì)和水分，分離出油和四氯乙烯的溶液，測(cè)定總萃取物含油量。同時(shí)可以將萃取液用硅酸鎂吸附，經(jīng)脫除動(dòng)植物油等極性物質(zhì)后，測(cè)定石油類?？傒腿∥锖褪皖惖暮烤刹〝?shù)分別為2930cm-1（CH2基團(tuán)中C-H鍵的伸縮振動(dòng)）、2960cm-1（CH3基團(tuán)中C-H鍵的伸縮振動(dòng)）和3030cm-1（芳香環(huán)中C-H鍵的伸縮振動(dòng)）譜帶處的吸光度A2930、A2960和A3030進(jìn)行計(jì)算。動(dòng)植物油的含量按總萃取物與石油類含量之差計(jì)算。</div><div>　　便攜式紅外測(cè)油儀的操作步驟：</div><div>　　1.首先打開(kāi)便攜式紅外測(cè)油儀箱和前處理箱，用電源線連接前處理箱的蓄電池并打開(kāi)側(cè)面主機(jī)開(kāi)關(guān)，長(zhǎng)按6秒打開(kāi)8寸的平板電腦使儀器預(yù)熱5分鐘。然后打開(kāi)前處理萃取器檢查硅酸鎂瓶，無(wú)水硫酸鈉瓶，鹽酸瓶，三角瓶，量筒，采樣萃取瓶，萃取活塞，四氯乙烯瓶，萃取器，比色皿是否完好可用，準(zhǔn)備采樣。</div><div>　　2.打開(kāi)電腦的便攜紅外測(cè)油儀的工作站，點(diǎn)擊進(jìn)入樣品測(cè)試頁(yè)面，從前處理設(shè)備箱取出四氯乙烯和比色皿清洗比色皿2次，再加入空白四氯乙烯放入比色池并點(diǎn)擊空白歸零?？瞻壮鰣D平滑無(wú)鋸齒即可。</div><div>　　3.將采樣萃取瓶加入攪拌子和鹽酸酸化到PH≤2，如果要出石油類的值那么再加入5勺硅酸鎂，然后蓋上萃取活塞，放到萃取器上設(shè)置萃取時(shí)間6-10分鐘左右，萃取完后自動(dòng)停止（水樣加入硅酸鎂后萃取時(shí)間須加長(zhǎng)，如果不加長(zhǎng)須在倒有萃取液的三角瓶再加入硅酸鎂和攪拌子放到萃取器上進(jìn)行攪拌吸附動(dòng)植物油）；如果要做動(dòng)植物油須先萃取，先測(cè)總油，然后再加入硅酸鎂和攪拌子放到萃取器上面進(jìn)行攪拌吸附動(dòng)植物油，設(shè)置時(shí)間20分鐘，自動(dòng)停止后測(cè)石油類，兩者相減即動(dòng)植物油。</div><div>　　4.萃取完后等待靜止分層約2分鐘左右，將采樣萃取瓶倒置打開(kāi)萃取活塞將樣品放入到加有3g左右無(wú)水硫酸鈉的三角瓶中，手動(dòng)搖勻無(wú)結(jié)晶即可（有結(jié)晶須再加入少量到不結(jié)晶為止），萃取溶劑不結(jié)晶后即可加入到比色皿進(jìn)行樣品測(cè)量，測(cè)量前將樣品的體積和四氯乙烯的體積填入固定的框中即可直接在軟件上讀取水中油類的濃度或石油類的濃度。</div> 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